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The chemistry of the Claus process involves partial oxidation of hydrogen sulfide to sulfur dioxide and the catalytically promoted reaction of hydrogen sulfide and sulfur dioxide to produce elemental sulfur. The reactions are staged and are as follows: Thermal stage: H2S + 3/2 O2 SO2 + H2O Thermal and catalytic stage: SO2 + 2H2S 3S + 2H2O The efficiency of sulfur recovery depends upon such things as feed composition, age of the catalyst, and number of reactor stages. Typical sulfur recovery efficiencies for Claus plants are 90 to 96 percent for a two-stage plant and 95 to 98 percent for a three-stage plant. Because of equilibrium limitations and other sulfur losses, overall sulfur recovery efficiency in a Claus unit usually does not exceed 98 percent. The off-gas leaving a Claus plant is referred to as tail gas, and, in the past was burned to convert the unreacted hydrogen sulfide to sulfur dioxide, before discharge to the atmosphere, which has a much higher toxic limit. However, the increasing standards of efficiency required by the pressure from environmental protection has led to the development of a large number of Claus tail gas clean-up units, based on different concepts, in order to remove the last remaining sulfur species (Gall and Gadelle, 2003). The oxygen-blown Claus process was originally developed to increase capacity at existing conventional Claus plants and to increase flame temperatures of gases having low hydrogen sulfide content. The process has also been used to provide the capacity and operating flexibility for sulfur plants where the feed gas is variable in flow and composition such as often found in refineries. Liquid redox sulfur recovery processes are liquid-phase oxidation processes which use a dilute aqueous solution of iron or vanadium to remove hydrogen sulfide selectively by chemical absorption from sour gas streams. These processes can be used on relatively small or dilute hydrogen sulfide stream to recover sulfur from the acid gas stream or, in some cases, they can be used in place of an acid gas removal process. The mildly alkaline lean liquid scrubs the hydrogen sulfide from the inlet gas stream, and the catalyst oxidizes the hydrogen sulfide to elemental sulfur. The reduced catalyst is regenerated by contact with air in the oxidizer(s). Sulfur is removed from the solution by flotation or settling, depending on the process. The wet oxidation processes are based on reduction-oxidation (redox) chemistry to oxidize the hydrogen sulfide to elemental sulfur in an alkaline solution containing an oxygen carrier. Vanadium and iron are the two oxygen carriers that are used. The best example of a process using the vanadium carrier is the Stretford process. The most prominent examples of the processes using iron as a carrier are the LO-CAT process and the SulFerox process. Both processes are capable of up to 99 percent or more sulfur recovery. However, using the processes for Claus tail gas treating requires hydrolysis of all the sulfur dioxide in the tail gas to hydrogen sulfide because the sulfur dioxide will react with the buffering base potassium hydroxide (KOH) and form potassium sulfate (K2SO4) which will consume the buffering solution and quickly saturate it. Tail gas-treating process involves the removal of the remaining sulfur compounds from gases remaining after sulfur recovery. Tail gas from a typical Claus process, whether a conventional Claus or one of the extended versions of the process, usually contains small but varying quantities of carbonyl sulfide, carbon disulfide, hydrogen sulfide, and sulfur dioxide as well as sulfur vapor. In addition, there may be hydrogen, carbon monoxide, and carbon dioxide in the tail gas.
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The word volatile used in this sense is intentional. It means the data changes and is not guaranteed to remain any particular value for any length of time.
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In this chapter, we covered the features of Windows Small Business Server 2003 that give it a flexible, robust, and recoverable storage system. With a pure NTFS file system as a requirement, Windows Small Business Server uses volume shadow copies, disk quotas, and file and folder encryption the tools for handling the storage needs of your business. In the next chapter, we ll cover users, groups, and managing the security and accounts of your Windows Small Business Server.
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almost exclusively by events in the tubular epithelium rather than the vascular endothelium; second, the cortical interstitium, which is the medium faced by the basolateral membranes of the tubular epithelia, has an osmolality and concentration of small solutes close to those in plasma. The interstitial composition changes when plasma composition changes. In the medulla, where both blood flow and transport events are quantitatively lower, things are far more complicated. Only some regions of the vasculature are fenestrated, so that (1) the overall transport depends on both the properties of the vascular endothelium and tubular epithelium, and (2) the medullary interstitium is most definitely not plasma-like in its composition. We will address the importance of these medullary properties later. For now, we direct our attention in the rest of this chapter to epithelial transport. Crossing the tubular epithelium can be performed in a single step or two steps. The paracellular route (single step) is when the substance goes around the cells (ie, through the matrix of the tight junctions that link each epithelial cell to its neighbor). More often, however, a substance goes through the cells, a two-step process: across the apical membrane facing the tubular lumen and across the basolateral membrane facing the interstitium. This is called the transcellular route. These structures and pathways are depicted in Figures 4 1A and B. An array of mechanisms exists by which substances cross the various barriers. The general classes of mechanisms are no different from those used elsewhere in the body to transport substances across cell membranes. We can view these mechanisms as a physiological tool box. Renal cells use whichever set of tools is most suitable for the task. The general classes of mechanisms for traversing the barriers are depicted in Figure 4 2.
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When we do a hypothesis test as described in the previous section, we never really know if we have made the correct decision or not. We can try to minimize our chances of being wrong, but there are trade-offs involved. If we are given a hypothesis, it may be true or it may be false. We can decide to reject the hypothesis or not to reject it. This leads to four possible outcomes:
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Conlin, VP of marketing at Incentive Systems in Bedford, Massachusetts. Conlin says he is often asked questions such as: What convinced you to come to Incentive Systems What are some of the best attributes of Incentive Systems Behavioral questions very similar to the type candidates are asked are also fair game to ask the interviewer, says Melanie Mays, president of Empyrean Consulting, a recruiting consulting firm in Dallas, Texas. These questions are best asked after a mutual interest has been established. They should go only to the individual with whom you might be working: Can you tell me about a project that was successful and how you accomplished it as a team Can you tell me about a time when you encountered constraints and how you resolved them How do you think your employees would describe your management style Some hiring managers are perfectly comfortable with such questions, but others might get defensive, Mays warns. If that s the case, back off, although the defensiveness itself will give you a clue about the situation. Other personal questions to consider asking the interviewer: Tell me about your career choice. How did you get into recruiting What attracted you to this organization What are some of the things you especially admire about the company If you could change some things about the company, what would they be How many layers of management are there between you and the CEO When was the last time you had contact with the CEO Avoid questions that are over the line. Personal questions that are clearly inappropriate would be ones such as: Are you single
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